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Ludwigshafen, Germany

How to simulate crystallization + granulation finishing

A continuous MSMPR crystallizer, cake filter, and dryer feed a granulator that grows the dried crystals into free-flowing granules — the finished-product train after the mother liquor and dryer vapor leave.

Featured in:Battery Metals
FEED
feed
solid
liq
CR
solid
liquor
cake
filt
FIL
wet
dry
vap
DRY
GRAN
FILT
VAP
Granules
  1. 1
    Open the ready-made model

    Open the "Crystallization + granulation finishing" model in the MaximaLabs workspace — no install, no license. It loads live on the canvas, ready to edit and run.

  2. 2
    Confirm the thermodynamics

    This process is modeled with the NRTL property package over ethanol, water — already selected, so the phase equilibrium and enthalpy are physically consistent from the first run.

  3. 3
    Review the flowsheet

    The flowsheet chains CR, FIL, DRY, GRAN. Every block is a real, solvable unit op you can reconfigure on the canvas.

  4. 4
    Run the simulation

    Click Run. The deterministic solver converges the material and energy balances (recycles included) and fills the live stream table — the AI never invents a number.

  5. 5
    Read the results and iterate

    Inspect the converged streams, tweak a spec, and re-run — or ask the AI copilot to explain a result or diagnose a failed solve in plain English.

What you'll build
Thermodynamics
NRTL
Components
ethanol, water
Unit operations
CRFILDRYGRAN
Open this model in the workspace

Opens live on the canvas — free, no install.

Explore the model & flowsheet

Frequently asked questions

What does the Crystallization + granulation finishing model simulate?
A continuous MSMPR crystallizer, cake filter, and dryer feed a granulator that grows the dried crystals into free-flowing granules — the finished-product train after the mother liquor and dryer vapor leave.
Which thermodynamic method does it use?
The NRTL property package, over ethanol, water — already selected. You can switch the method on the canvas before running.
Which unit operations are in the flowsheet?
It chains CR, FIL, DRY, GRAN. Every block is a real, solvable unit operation you can reconfigure, add to, or remove.
Do I need to install software or buy a license?
No. Crystallization + granulation finishing runs entirely in your browser on MaximaLabs — free, no install, no license. Open the model to load it live and run the deterministic solver.

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Crystallize → thicken (dewatering)

An MSMPR crystallizer precipitates the salt, then a gravity thickener dewaters the crystal slurry into a dense underflow while a clarified overflow leaves the top — the solid-liquid separation a hydrometallurgy plant runs before filtration.

Antwerp, Belgium

Solids train (crystallize → filter → dry)

An MSMPR crystallizer feeds a cake filter and dryer — the crystal size and cake moisture propagate on the stream's solids payload (pharma / minerals workflow).

Pharmaceutical crystallization / API finishing, Cork, Ireland

Crystallization with agglomeration (distributed CSD)

An MSMPR crystallizer solved with the rigorous distributed population balance (not just moments): the full crystal-size distribution is computed on a size grid, and an agglomeration (aggregation) kernel combines fine crystals into larger ones — coarsening the mass-weighted mean size (d43) and broadening the distribution (CV rises above the growth-only MSMPR value of ~1.0) while conserving mass exactly. The distribution, its coefficient of variation, and d43 propagate on the solid stream into the filter and dryer — the gPROMS/gCRYSTAL capability the moment model structurally cannot provide.

Reference model

Grinding-circuit hydrocyclone classifier

A hydrocyclone classifies a mineral slurry by particle size — the unit that closes every closed-circuit grinding loop (mill → cyclone, coarse underflow recycled to the mill). A quartz slurry (200 µm mean, spread by a log-normal PSD) is split about a 100 µm corrected cut size (Plitt 1976): the coarse solids report to the thick underflow and the fines to the dilute overflow, split by the short-circuit recovery. The underflow comes out much coarser (~300 µm mean) than the overflow (~80 µm), and the solids mass balance closes exactly. Honest scope: the d50c is the real Plitt correlation, but the partition sharpness and water recovery are screening params.

Murrin Murrin nickel-cobalt laterite operation, Western Australia

Cobalt/nickel solvent extraction (D2EHPA)

A laterite leach liquor (Co/Ni/Mg in dilute sulfate solution) meets a D2EHPA-in-kerosene organic phase across a 20-stage countercurrent extraction circuit run at pH 5.2 — the real industrial operating window (e.g. Bulong, Murrin Murrin, Western Australia) that exploits the ~1 pH-unit gap between Co and Ni's D2EHPA extraction isotherms: Co extracts into the organic while Ni (and Mg gangue) are rejected to the raffinate. The loaded organic then meets fresh dilute-acid strip liquor across a 10-stage strip circuit at pH 1.0 (well below Co's isotherm), reversing the equilibrium to recover a concentrated cobalt strip liquor and regenerate barren organic. Real pH-isotherm chemistry throughout, not a fitted shortcut K_D.

Salar de Atacama, Chile

Direct lithium extraction + LiOH crystallization

A Salar-brine DLE train: an Al-based sorbent column selectively loads Li+ (rejecting the brine's much larger Mg2+ background — real DLE sorbents cut a ~290:1 Mg/Li mass ratio down to under 1:1), the loaded sorbent is eluted with fresh water into an aqueous strip liquor (bridging the sorption column's own documented single-pass-loading scope), RO concentrates it, a real bipolar-membrane electrodialysis (BPED) cell converts LiCl to LiOH — Faraday's law links the applied current/membrane area/current efficiency to the actual Li+ transport rate (replacing an earlier placeholder fixed-conversion reactor), reporting real cell voltage and electrical power draw — and a forward-feed two-effect evaporator train (vapor from effect 1 heats effect 2) concentrates it to battery-grade LiOH·H₂O crystals. Real boiling-point elevation throughout via the Pitzer-electrolyte brine thermo package. Isotherm parameters per the sorption column's own citation (2024 Desalination study, Al-based DLE sorbent).

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