MaximaLabs

A PDH cold box, where the propylene is actually lost

Propane dehydrogenated to propylene over a Pt/Cr catalyst, then recovered cryogenically from the hydrogen-rich reactor off-gas.

Reaction and cryogenic recovery on one flowsheetAfter US Patent 6,333,445 (Chart Inc., 2002)Cold box as a net duty — stated, not disguised
Propane feed
PDH reactor
Cold box
Separator
Liquid propylene
H₂-rich off-gas

The actual dark-mode canvas: propane dehydrogenated over a Pt/Cr catalyst, then the reactor effluent chilled in a cold box so propylene condenses out and the hydrogen leaves as off-gas.

Where the propylene is actually lost

Dehydrogenation is equilibrium-limited, so per-pass conversion is modest and the recovery step decides the economics — every degree the cold box misses sends propylene out with the hydrogen. Scope note: the refrigeration loop itself is not modelled here; the cold box is represented as the net cooling duty required, which the example's description states plainly.

C3H8C3H6+H2(endothermic, equilibrium-limited)\mathrm{C_3H_8} \rightleftharpoons \mathrm{C_3H_6} + \mathrm{H_2} \quad \text{(endothermic, equilibrium-limited)}
recovery=1yC3H6VzC3H6F(set by the cold-box temperature)\text{recovery} = 1 - \frac{y_{\mathrm{C_3H_6}}\,V}{z_{\mathrm{C_3H_6}}\,F} \quad \text{(set by the cold-box temperature)}
KH2KC3H6(why a single cold flash separates them cleanly)K_{\mathrm{H_2}} \ggg K_{\mathrm{C_3H_6}} \quad \text{(why a single cold flash separates them cleanly)}

Unit ops shipped for this vertical

Fixed-conversion reactor

A specified per-pass conversion on a key component — the shortcut counterpart to the equilibrium and kinetic reactors.

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Heater / cooler

Duty- or outlet-condition-specified energy-balance stage.

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Flash drum

Single-stage vapor-liquid equilibrium split at a fixed temperature/pressure.

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Live plant integration

Stream reactor conversion and cold-box outlet temperature from the unit's OPC-UA server into this flowsheet's twin comparison — propylene recovery is a steep function of that temperature, so a small drift is a large loss.

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Try it yourself

  • Reaction and cryogenic recovery on one flowsheet
  • After US Patent 6,333,445 (Chart Inc., 2002)
  • Cold box as a net duty — stated plainly, not disguised

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