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Alkylation Process Flowsheets & Simulations

Explore 5 validated, solved Alkylation simulation flowsheets in MaximaLabs — real components: phenol, methanol, o_cresol, 2_6_xylenol, water, ethylene. Open any one directly in your browser.

Solved via: PENG-ROBINSON.

Phenol FEED
Methanol FEED
MIX
Meth1
Meth2
crude
dist
cuts
btms
COL
Methanol Water
O Cresol Product
Xylenol Product
Phenolics plant, Deer Park, Texas, USA

2,6-Xylenol from phenol methylation

Liquid-phase methylation of phenol with methanol at 250°C/150 bar over a selective ortho-methylation catalyst, per US Patent 3,707,569. At 50% single-pass phenol conversion the reported selectivity is 70% to o-cresol and 25% to 2,6-xylenol (the further-methylated product) — modeled here as two sequential fixed-conversion reactors (phenol -> o-cresol, then o-cresol -> 2,6-xylenol) approximating that split, followed by a distillation separating the light methanol/water from the phenolics. The five-component side-draw column sits in the same successive-substitution residual plateau documented for the light-ends-train and DME-synthesis examples — it returns a physically reasonable partial profile rather than a clean converged status.

9 unit ops • PENG-ROBINSON

17 0

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FEED
RX
COOL
feed
dist
btms
Bzcol
Light
EB
Styrene chain, Antwerp, Belgium

Ethylbenzene synthesis

Benzene alkylation with ethylene (exothermic, 98% ethylene conversion) followed by a recovery column — 100% EB bottoms. From the ChemSep casebook (AIChE J 57, 655).

6 unit ops • PENG-ROBINSON

17 0

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Benzene
Propylene
MIX
RXN
feed
dist
btms
COL
Benzene Recycle
Cumene Product
Reference model (Luyben 2010)

Cumene production (benzene alkylation)

Benzene and propylene alkylate over a fixed-conversion reactor to cumene (isopropylbenzene, the feedstock for phenol/acetone via the Hock process); a downstream column recovers unreacted benzene overhead for recycle-quality purity while cumene leaves the bottoms. Luyben, Ind. Eng. Chem. Res. 2010, 49, 719.

7 unit ops • PENG-ROBINSON

17 0

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Butene
Isobutane Makeup
MIX
RXN
feed
dist
btms
DIB
Alkylate
Reference model (Luyben 2009/2011)

Butene/isobutane alkylation

Sulfuric-acid alkylation of butene with excess isobutane produces high-octane alkylate gasoline blendstock; a conversion reactor stands in for the acid-catalyzed carbocation chemistry (a literal acid/hydrocarbon settler would need H2SO4 electrolyte thermodynamics this package doesn't carry — out of scope, same as the reactor already being a stand-in for the chemistry itself), and a deisobutanizer-style column recovers unreacted isobutane overhead. The high isobutane:olefin ratio real alkylation units run is maintained almost entirely by recycling that isobutane back to the reactor feed — closed here as a real Wegstein-converged tear loop, with only a small makeup feed replacing what the reaction actually consumes, rather than the previous version's isobutane leaving as an unrecycled product. Luyben, Principles and Case Studies of Simultaneous Design, Wiley (2011); Ind. Eng. Chem. Res. 2009, 48, 11081.

6 unit ops • PENG-ROBINSON

17 0

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FEED
Alkrx
COOL
feed
dist
btms
Alkcol
Light ENDS
Reheat
Dehydro
SEP
Offgas H2
feed
dist
btms
Stycol
Ethylbenzene Product
Styrene Product
Styrene chain, Antwerp, Belgium

Integrated styrene chain: benzene to styrene monomer

The full two-step styrene chain connected as one flowsheet rather than two standalone process snippets: benzene alkylated with ethylene to ethylbenzene, purified in a recovery column, then fed directly to the dehydrogenation reactor that makes styrene monomer. The unreacted ethylbenzene the dehydrogenation column recovers is reported as its own product stream rather than recycled back onto the alkylation feed (an honest simplification — closing that loop needs a torn-recycle edge back into ALKCOL, which the plant does but this flowsheet does not).

12 unit ops • PENG-ROBINSON

17 0

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