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Consecutive reactions Process Flowsheets & Simulations

Explore 2 validated, solved Consecutive reactions simulation flowsheets in MaximaLabs — real components: ethylene, oxygen, ethylene_oxide, co2, water, ethylene_glycol. Open any one directly in your browser.

Solved via: PENG-ROBINSON.

Ethylene FEED
O2 FEED
MIX0
Epoxrx
Combrx
Cool0
Condense
Purge GAS
Waterfeed
MIX1
RXN1
RXN2
RXN3
Cool1
Degas
Offgas
Dewater
Water Recycle
MEG COL
MEG Product
DEG COL
DEG Product
TEG Product
MEG/EG complex, Jubail, Saudi Arabia

Ethylene glycol plant: fiber-grade MEG + DEG/TEG byproducts

Extends the EO/glycol chain all the way to separated products. Ethylene + O₂ make ethylene oxide over a silver catalyst (with the competing total-combustion side reaction), EO condenses out, and then hydrates through the real CONSECUTIVE glycol reactions — EO + H₂O → MEG, EO + MEG → DEG, EO + DEG → TEG (all atom-balanced, keyed on the shrinking EO pool) — giving the industrial ~90/9/1 mono-/di-/tri-ethylene-glycol selectivity that a high water:EO ratio produces. The purification train recovers the water for recycle and splits the glycols into fiber-grade MEG (>=99.9%), DEG, and TEG products. HONEST SCOPE: the reaction chemistry is rigorous stoichiometry (real atom balances, realistic selectivity set by the fixed conversions); the PURIFICATION is modelled with spec-based component-split separators to the known product purities (the Aspen 'Sep'-block technique for a well-understood separation section), NOT rigorous vacuum distillation columns — a converged 99.9%-fiber-grade MEG column is not tractable in this solver under Peng-Robinson (the MEG/DEG relative volatility is too narrow for the wide-boiling MESH path; a real plant uses large multi-effect evaporators + vacuum columns). The water-recycle stream is left open (not looped back) — an honest simplification, like the parent EO example's ethylene recycle.

23 unit ops • PENG-ROBINSON

224 0

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NH3
Water
EO
MIX
RXN1
RXN2
RXN3
COOL
Ammstrip
NH3 Recycle
Dewater
Water OUT
Meacol
MEA Product
Deacol
DEA Product
TEA Product
Ethylene oxide / amines complex, Antwerp, Belgium

Ethanolamines plant: MEA / DEA / TEA from ethylene oxide + ammonia

The nitrogen analogue of the ethylene-glycol chain, and a major gas-treating-solvent process in its own right. Ethylene oxide reacts with ammonia through the same kind of CONSECUTIVE addition chain the glycols follow — EO + NH₃ → monoethanolamine (MEA), EO + MEA → diethanolamine (DEA), EO + DEA → triethanolamine (TEA), all atom-balanced and keyed on the shrinking EO pool. A large ammonia excess pushes selectivity toward MEA (the ~80/13/5 MEA/DEA/TEA slate a high NH₃:EO ratio makes, amine-side mirror of how a high water:EO ratio favours MEG). The separation strips the excess ammonia (recovered for recycle) and the reaction water, then splits the amines by boiling point (MEA 170 C < DEA 269 C < TEA 335 C) into ~99.8% MEA, high-purity DEA, and a TEA bottoms cut. HONEST SCOPE: the reaction chemistry is rigorous stoichiometry (real atom balances, realistic selectivity from the fixed conversions), and the amines are characterized as pseudo-components (Tc/Pc/omega from the open-data databank — MEA/DEA/TEA have no CoolProp entry) so they flash under Peng-Robinson. The purification uses spec-based component-split separators (the Aspen 'Sep'-block technique), NOT rigorous vacuum columns — the ethanolamines are wide-boiling with narrow adjacent-amine relative volatilities, the same wide-boiling-MESH limit measured for the glycol columns. The recovered ammonia is shown as an open recycle stream (an honest simplification, like the parent EO example).

17 unit ops • PENG-ROBINSON

220 2

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